Chris Blake - " My first day of work at the RSC was Monday December 1st 1975. All the RSC instruments used electromagnets with field strengths in which protons resonated at either 60 Mhz or 100 MHz. My first lesson in operating a spectrometer consisted of sitting at the console of a JEOL C60HL and being told to fiddle with all the knobs to see what they did. We had two pulsed instruments, the rest were continuous wave (CW). There were no computers involved with the CW instruments. The recorder arm moved slowly across the chart, taking about 3 minutes, drawing the spectrum as it went. The only storage of the result was the chart paper the spectrum was drawn on.
The way the NMR service operated was quite different in those days. Students would fill out an A4 paper form and submit it with their sample which was usually a powder. These would be placed in a pidgeon hole, and when the sample's turn came, the technician would add the deuterated solvent, make up the sample in an NMR tube, and run the spectrum. It was not until the creation of the "University NMR Centre" in 1984 that students were expected to operate the spectrometers themselves, however they were only allowed to "fly solo" after passing a practical test. The ANU had no financial problems in those days, so the staffing levels were relatively high. We had a tea lady, and the tea room was full to overflowing with staff and students twice a day."
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